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    Experimental study on the failure factors of the O-ring for long-term working①

    2023-09-12 07:29:46SUNYuantao孫遠(yuǎn)韜ZHANGMinYUANLindong
    High Technology Letters 2023年3期

    SUN Yuantao(孫遠(yuǎn)韜),ZHANG Min,YUAN Lindong

    (?School of Mechanical Engineering,Tongji University,Shanghai 200092,P.R.China)

    (??Metering Department,Shanghai,Fiorenti Gas Equipment CO,.LTD,Shanghai 201201,P.R.China)

    Abstract The O-ring in the rotary dynamic sealing system of gas meters should have outstanding longterm sealing performance under the conditions of high and low temperature,which can ensure the safety of gas meters.In this paper,based on the O-ring sealing mechanism,taking the compression set as the main sealing index, a finite element simulation method is used to analyze the failure characteristics under different conditions according to the constitutive relation of nitrile rubber.Then,using the orthogonal test method for the O-ring sealing performance index,the main factors which affect the law of long-term test are analysed,and the orthogonal regression mathematical model that can predict the compression set is obtained.Finally,the O-ring is improved according to the model,and the test results show that the performance of the new O-rings with high and low temperature resistance is greatly improved and meets the expected target requirements.

    Key words:NBR O-ring, compression set, rotary dynamic seal, orthogonal test, regression analysis

    0 Introduction

    O-ring is suitable for a variety of mechanical equipment,and can plays a sealing role in a static or moving state in specified temperatures,pressure,and different liquid and gas media.It is widely used in machine tools,ships,automobiles,aerospace equipment,machineries in industries,and various of instruments and meters.As the core component in the sealing system,once the O-ring fails,the light will lead to sealing media leakage,equipment can not work properly or even cause serious accidents.

    For gas meters,in order to ensure the accuracy of measurement and gas safety, the long-term sealing method of gas meters must be reliable.Among several mainstream gas meters sealing methods,the O-ring seal is the most widely used one.Nitrile rubber (hereinafter referred to as NBR) is the most common O-ring material due to its good mechanical properties,resistance to lubricants and grease,and relatively low cost[1].It is valuable to study the long-lasting sealing performance of the sealing system of the NBR O-ring rotary dynamic sealing system for gas meters,both from the perspective of safe gas use and life time requirements.

    In terms of O-ring failure indicators,Ref.[2]conducted long-term tests of O-rings to predict the service life of packages used for long-term cross section,to reduce strain energy,and monitoring of storage,and their preliminary data suggests that CSR (compressive stress relaxation) data are valuable for predicting the service life of O-rings when there is no leakage.Ref.[3] studied the dynamic and static sealing performance of O-rings using a specially designed test device,and concluded that the O-ring compression set can be used as an important index to evaluate its sealing performance.

    For O-ring dynamic sealing performance studies,Ref.[4]predicted the life and reliability of O-rings by non-destructive tests (e.g.Shore a hardness measurements) and used them to aid decision making.A twodimensional axisymmetric computational fluid dynamics(CFD) model was preprocessed in GAMBIT of Ref.[5],and heat transfer analysis was performed using FLUENT to investigate the variation of frictional torque,O-ring frictional power loss,and interface temperature with sliding velocity and operating differential pressure.The results show that the power loss of the Oring increases roughly linearly with the increase in sliding speed[5].Ref.[6] investigated the design of O-ring cross-sections,which include small embedded regions with different material behavior among the surrounding large the compression set, and time-varying load deformation behavior of the specimens showed that the amount of compression set is related to the strain energy,while the compression set of the material affects the performance of the structure.Ref.[7] performed rapid measurements of various parameters affecting the dynamic performance of O-rings,including O-ring stiffness and damping coefficient,through test procedures.In order to investigate the effects of extrusion and pressure on the dynamic properties of NBR and fluorocarbon O-rings,tests were conducted and it was concluded that increasing the level of extrusion or system pressure increased the stiffness and damping coefficient, as well as the size of the O-ring cross-sectional diameter had little effect on the stiffness and damping coefficient.Ref.[8] studied the performance of O-ring reciprocating dynamic seals in hydraulic systems and analyzed the effect of different stresses and design parameters on contact pressure with finite element software to obtain the degree of influence of applied stresses and seal structure design parameters on the sealing performance of O-rings.

    For the selection of test methods,Ref.[9] designed a procedure applicable to the characterization of deformation behavior of various engineering materials during processing.The procedure used orthogonal processing tests to obtain the relationships between shear stress,strain,strain rate,and temperature.A novel constitutive model for mild steel determined by this procedure was proposed with the help of the orthogonal test method.Ref.[10] used the orthogonal experimental method to reduce the number of experiments and determine the key parameters in the relevant experiments,and divided the nine parameters into three groups,including printing parameters, temperature parameters and structural parameters.The three groups of experiments were investigated separately to determine the effects of factors on the mechanical properties of shape memory polymer (SMP) samples,and the optimal combination of temperature and printing parameters for SMP printing and the effect of structural parameters on the tensile strength of the specimens were determined.This experimental study involves three factors and three levels,in order to better analyze the effects of time,rotational speed and temperature on the compression set of the sealing index and its corresponding sealing effect,and because the time of this experimental study is too long,this paper will design the orthogonal test with three factors of time,temperature and rotational speed for the study,which can greatly shorten the test time and at the same time ensure the validity of the test results.

    In summary,at present,research on the sealing performance of NBR O-ring in sealing system mainly focuses on the O-ring itself (such as aging index,static sealing performance, dynamic sealing performance)and the performance of NBR original material (such as material life,intrinsic model selection),and lacks a comprehensive research analysis combining simulation and actual life cycle test on the O-ring rotary dynamic sealing system from the perspective of sealing failure factors[11-14].In this paper,the failure characteristics of the O-ring is analyzed under different working conditions by using the finite element simulation method based on the intrinsic structure relationship of nitrile rubber for the compression set,and on this basis,we conduct long-term tests and analysis on the sealing performance indexes and the influence law of the main influencing factors of the O-ring by orthogonal test method,and obtain the orthogonal regression mathematical model that can predict the compression set and finally improve the O-ring according to this model.

    1 NBR O-ring rotary dynamic sealing system finite element analysis

    1.1 Introduction to structure of the O-ring sealing system

    As shown in Fig.1,the rotary sealing system consists of an O-ring,a split washer,a linkage shaft,a linkage bushing,and a linkage shaft seat,with the Oring near the split washer side being the inside of the meter body,i.e.,the side that bears the pressure of the medium,and the other side being the outside of the meter body.The gap between the linkage shaft and the linkage shaft seat is sealed in both directions by the Oring,isolating the inside of the meter body from the outside of the meter.During the ventilation work,the male crank drives the linkage flag to rotate,thus making the linkage shaft rotate and transfer the gas volume to the counter to meter.

    Among the main causes of O-ring failure in sealing systems[15],the reduction of seal overfill caused by the compression set is an important cause of seal failure[3],and at the same time,the compression set can be observed and measured visually,qualitatively and quantitatively,so this paper selects the index of the compression set of the O-ring to study its sealing performance.

    Fig.1 O-ring rotary dynamic sealing system structure diagram

    The O-ring is mainly subjected to shear stress,contact stress and Von Mises stress in the sealing system,which lead to compression set.Therefore,the effect of temperature and rotational speed on these three forces can reflect the effect of temperature and rotational speed on the compression set of O-rings to a certain extent.Considering that the mechanical results in ABAQUS are more accurate and easier to obtain than the compression set, the above three forces are chosen to represent the compression set to a certain extent in the simulation experiment.

    This finite element analysis which is established a finite element model in ABAQUS,according to the simulation experimental protocol,through the analysis of the above three stresses under different working conditions,can obtain the results of the force of the O-ring in the sealing system under the composite factors and meanwhile deduce the degree of influence of each factor alone on the O-ring in the sealing system,thus to predict the possible compression permanent deformation area[16-18].

    The Mooney-Rivlin model has been validated for finite element mechanical analysis of rubber materials,especially for small and medium deformations,and is a good fit for the O-ring in this study.The calculated deformation,damage and other failure forms of the O-ring during the simulated stress analysis of the O-ring sealing system will be closer to the actual test results[19-21].The 3D model of the rotating dynamic sealing system in this study is modeled using SOLIDWORKS,the 3D model is simplified in ABAQUS,which is easy to converge the simulation results,as shown in Fig.2; the 3D stress linear cell C3D8R is used to mesh the model in ABAQUS[22-25],the established O-ring model is shown in Fig.3.

    Other pre-processing steps of FEA are as follows:(1) Set the pre-compression of O-ring to 15%[26];(2) Set the temperature field according to the working condition; (3) Apply 2 kPa working medium pressure to the seal to complete the static sealing process; (4)Apply two reverse rotational velocities to the shaft barrel to simulate the rotational motion process,and the velocity size will be changed according to the working condition.

    Fig.3 Drawing of the 3D O-ring mesh model

    The simulation test factors are temperature,rotational speed and pressure.The operating pressure is fixed at 2 kPa,and the temperature is set as -25 ℃,20 ℃and 60 ℃; according to the working principle of the membrane gas meter used in this study,the rotational speed is 86 r/min when the gas flow rateq=6 m2/h,and 58 r/min whenq=4 m2/h,so the test rotational speed is 86 r/min,58 r/min and 0 r/min.The two-factor,three-level full-scale experimental protocol for temperature and speed is shown in Table 1.

    Temperature RPM B1( -25 ℃) B2(20 ℃) B3(60 ℃)A1(86 r/min) A1B1 A1B2 A1B3 A2(58 r/min) A2B1 A2B2 A2B3 A3(0) A3B1 A3B2 A3B3

    1.2 Simulation experiment results and data analysis

    Simulation analysis was performed for each of the nine scenarios according to Table 1.ABAQUS was applied to set up the load scenarios by experimental protocol,and numerical simulations were performed to analyze and output force clouds and data as required[27-30],where the results of Scenario 1 are shown in Fig.4,and the results of the other eight scenarios are shown in Appendix I( limited to space).

    (1)A comparison of the average Von Mises stress data for the nine scenarios is shown in Fig.5.From Fig.5,it can be seen that the Von Mises stress of the O-ring and does not vary much increases with increasing temperature in the dynamic seal state; the stress value does not vary much at different rotational speeds;in the static seal state,does not vary much with decreasing temperature.The Von Mises stress is not sensitive to temperature, does not vary much between different rotational speeds, and varies greatly between dynamic and static.

    (2)A comparison of the average contact stress data for the nine scenarios is shown in Fig.6.As can be seen from Fig.6,the contact stress of the O-ring,which increases with temperature,varies greatly; the stress values at different rotational speeds are relatively close and do not vary much.Contact stress is more sensitive to temperature and has a good effect; the speed has a relatively small effect on contact stress.

    (3) The average shear stress data comparison is shown in Fig.7.As can be seen from Fig.7,the shear stress CSHEAR 1 and CSHEAR 2 of the O-ring,increases with temperature in the dynamic seal condition; in the static seal condition,the stress decreases with temperature and both vary greatly.The difference in stress values between dynamic and static seals is large,and the stress values at different rotational speeds are relatively close and do not vary much.Shear stress is more sensitive to temperature and has a significant effect; rotational speed has a relatively small effect on contact stress.

    Fig.5 Average Von Mises stress comparison

    Through finite element analysis,the results of the influence of temperature and rotational speed on the three stresses were obtained as follows.

    (1) Von Mises stresses vary little at different temperatures (the maximum of variation is at 58 r/min:3%),the response is not obvious; contact stresses and shear stresses vary much at different temperatures(contact stresses: 13.73% at 58 r/min; CSHEAR1:-22.29% at 0 r/min; CSHEAR2: - 28.36% at 0 r/min),the response is obvious.

    (2) Von Mises stresses,contact stresses and shear stresses vary little at different speeds under dynamic seal condition ( Von Mises stresses:0.0143% at 20 ℃; Contact stresses: 0.0154% at-25 ℃; CSHERA 1: 0.00357% at 20 ℃;CSHERA 2: 0.0392% at-25 ℃),the response is not obvious.

    (3) Whether the seal state is static or not has a significant effect on Von Mises stresses and shear stresses,while it is not significant for contact stresses.And because the permanent compression deformation of O-ring depends on the above three stresses,it can be seen that the temperature has the greatest influence on the sealing performance of O-ring,followed by the speed.

    2 Experimental study of the NBR O-ring rotary dynamic sealing system

    In this test,air was used as the medium for the ventilation and sealing test to simulate as much as possible the conditions of the O-ring during the actual operation of the gas meter.At the end of the test,an underwater devices for detecting seal ability was used to test that if there was no leakage within 1 min[31],the O-ring sealing performance was considered to meet the requirements.The O-ring that completed the test was taken out and its dimensions were measured and the data were analyzed and the compression setCf≤50%at-25 ℃,20 ℃andCf≤40% at 60 ℃were considered to meet the requirements,and vice versa[29].

    The compression set measurement method is based on ISO 815-1[32],and the compression set rate is calculated by Eq.(1) to quantitatively evaluate the amount of compression set as follows.

    whereCfis amount of compression set of the O-ring in compression,d0is O-ring original section diameter,dfis O-ring section diameter after the compression,anddcis thickness of the O-ring under compression.

    2.1 Experimental protocol

    In the study,the three factors(time,temperature and speed)were set as follows.

    (1)Time:2000 h,3500 h,6000 h

    2000 h and 3500 h are the stage tests in the 5000 h endurance test,and at the same time,2000 h is the minimum endurance test requirement to be met by the gas meter; the upper limit of 6000 h is selected to have higher performance requirements for the sealing system,while the interval range covers 5000 h,so that the model obtained from the test can cover the range of 2000 h to 6000 h.

    (2)Temperature:-25 ℃,20 ℃,60 ℃

    20 ℃is the room temperature;-25 ℃and 60 ℃are the higher requirements for high and low temperature working environment of gas meters.

    (3)Speed:86 r/min,58 r/min,0 r/min

    The maximum flow rate of the gas meter is 6 m3/h,which corresponds to the rotational speed of 86 r/min;the most common flow rate of the gas meter is 4 m3/h,which corresponds to the rotational speed of 58 r/min,and the state of rotational speed of 0 r/min under 0 flow rate.

    The orthogonal test protocol is shown in Table 2[33-34].

    Num Factors Time/h Temperature/ ℃ RPM 1 2000 -25 58 2 2000 20 86 3 2000 60 0 4 3500 60 86 5 3500 20 58 6 3500 -25 0 7 6000 20 0 8 6000 -25 58 9 6000 60 86

    There are 9 groups of tests,and each group needs to test 6 gas meters,i.e.6 O-rings.

    2.2 Test environment and equipment

    (1)Test environment

    Temperature:20 ±2 ℃;

    Relative humidity:35% -75% RH;

    Atmospheric pressure:86 -106 kPa;

    Medium: air.

    (2) Testing device

    1) Endurance test device: it consists of profile bracket,speed control fan,pipeline and gas meter,where each fan drives two gas meters,the flow rate is controlled by the speed of rotation of the roller counter in gas meter,regulating the actual flow rate of 6 m3/h(86 r/min),4 m3/h (58 r/min).The working principle of the endurance device is shown in Fig.8.

    Fig.8 Schematic of the endurance test device

    2) Gas meter sealing testing device: it is made up of gas pipeline,pressure gauge,cylinder,lifting mechanism,water tank.Test pressure can be adjusted by turning the knob manually.

    3) Digital projector,high- and low-temperature test chamber,experimental meters,etc.,see Appendix II for details.

    2.3 Results of the orthogonal test

    After completing 9 scenarios in accordance with the orthogonal test protocol,the performance of the Oring rotary dynamic sealing system was tested by the water test method with the seal testing device; after the test,the O-ring sealing system sealing test was all qualified,and in terms of the test O-ring,the O-ring longterm sealing performance was proved to be reliable.The testing process is shown in Fig.9.

    Fig.9 Diagram of the gas meter sealing test process

    After the experiments were completed,six gas meters in each of the nine groups were disassembled,the deformed O-rings were removed,and their section diameters and overall internal diameters were measured using a projector.It was found that the O-rings had obvious compression set in the radial direction by compression.Before data processing,the section diameters and overall inner diameters of the six O-rings of the same batch that were not used were measured in advance as initial values.After obtaining the O-ring dimension data,the measured data were handled according to Eq.(1) to obtain the compression set data,and the rangeRwas calculated according to the three-factor,three-level orthogonal table data processing method,and the test data are shown in Table 3.[35-36]

    Average compression set 1 2000 -25 58 44.81%2 2000 20 86 20.83%3 2000 60 0 23.43%4 3500 60 86 39.50%5 3500 20 58 21.48%6 3500 -25 0 27.91%7 6000 20 0 16.28%8 6000 -25 58 61.29%9 6000 60 86 56.22%K1 0.8907 1.3401 1.1655 K2 0.8889 0.5859 1.2758 K3 1.3379 1.1915 0.6762 k1 0.2969 0.4467 0.3885 k2 0.2963 0.1953 0.4253 k3 0.4460 0.3972 0.2254 range R 0.1497 0.2514 0.1999 Num Factors Time/h Temperature/ ℃ RPM

    2.3.1 Intuitive analysis method

    To distinguish the primary and secondary factors of the test,as well as to determine the significance of the influence of each factor on the test indexes,intuitive analysis was first used to obtain the results as shown in Fig.10 based on the data in Table 3.

    Fig.10 Intuitive analysis

    From Fig.10,it can be intuitively seen that the value of the largest range of variation is factorB,factorCranks second,and factorAis the most inferior,so it can be judged that the degree of influence of these three factors on the compression set of compression is:factorB> factorC> factorA,that is,the temperature factor has the greatest influence,followed by the speed factor,and the time factor has the least influence.

    2.3.2 Analysis of variance (ANOVA) method

    To obtain more precise analysis results,the data was then further processed by ANOVA to obtain the degree of significance of the effects of different factors.The experimental data were calculated using a threefactor ANOVA using the Matlab ANOVA formula[37-40],and the results are shown in Table 4,where,SSis variance,Dfis degree of freedom,MSis mean squared error,Fdenotes F-value,andProb>Fdenotes P-value.The F-test was performed on the ANOVA,and from Table 4,it can be concluded that the P-values of factorB,and factorCare less than 0.01,and both reject the H0 hypothesis,so both factors have a significant effect on the compression set atα=0.01 significance level; and since the P-value of factorBis smaller,so between the two factors,factorBhas a greater effect and factorCis the second.The effect of factorAwas not significant atα=0.01 significance level.That is,among the three factors,temperature has the greatest effect on compression set,rotational speed is the second and time is the third.This conclusion is consistent with the results obtained from the previous finite element simulation and the two can corroborate each other.

    Source SS Df MS F Prob>F Factor A 0.044 62 2 0.022 31 80.50 0.0123 Factor B 0.104 42 2 0.252 21 188.37 0.0053 Factor C 0.065 91 2 0.032 96 118.91 0.0083 Error 0.000 55 2 0.000 28 Sum 0.217 49 8

    2.4 Orthogonal fit regression analysis of experimental data

    To maximize the effect of the results of this test,regression analysis was performed on the compression set data to obtain a prediction model of the relationship between three factors: time, temperature, rotational speed,and the compression set of the O-ring.To facilitate the calculation of the whole data analysis process,before proceeding to analyze the data,the data were processed in advance using normalization methods to avoid the problem of inconsistent physical meaning of each data parameter[41-43].The following quadratic polynomial response model for the fitted and estimated amounts of compressive compression set,Eq.(2) is developed.

    where,x1denotes time factorA;x2denotes temperature factorB;x3denotes speed factorC;adenotes the constant term;b1-b3denotes the primary term coefficients;b4-b9denotes the secondary term coefficients;εdenotes the model error.

    The data in Table 2 are normalized by using Matlab and substituted into Eq.(2) together with the data in Table 3 for compression set,and the response model coefficients are solved by least squares method with the help of Matlab[44-45],and the quadratic polynomial response model Eq.(3) for the compression set target can be obtained by substituting the normalized model coefficient values into Eq.(1).

    2.5 Model fitting accuracy test and prediction test validation

    2.5.1 Model fitting accuracy test

    The coefficient of determinationR2is used as the evaluation index model for the accuracy fitting test,which is defined in Eq.(4).

    R2=0.8840,which exceeds 0.8,shows that the model fits well and that this compression permanent variable response model has high accuracy.

    2.5.2 Test verification

    The prediction model of the compression set of Oring was tested and verified: according to the same conditions of the previous orthogonal test,a group (6 units) of gas meters was arranged,the time was set to 5000 h,the temperature was 20 ℃,and the speed was 86 r/min.After the test was completed,the O-ring samples were taken out,their dimensions were measured with a projector,and the data were obtained and calculated according to Eq.(1).Their average compression set was 30.89%,which was compared with the predicted value of 33.61% given by the normalized quadratic polynomial prediction model,and the error value was 8.81%,indicating that the results of the prediction model had a small error value with the test data,and the relative accuracy was high.

    3 NBR O-ring rotary dynamic seal performance improvement and application

    The previous experimental study verified that the sealing performance of the O-ring met the requirements,but by Table 5,it can be seen that: dynamic sealing system O-ring in-25 ℃low temperature state,after 2000 h of continuous work,its compression set value reached 44.81%,close to 50%; after 6000 h of continuous work,the compression set value reached 61.29%,more than 50%,the indicator does not meet the requirements; dynamic sealing system O-ring in 60 ℃high temperature state,after 3500 h of continuous work,its compression set value reached 39.50%,close to 40%; after 6000 h of continuous work,the compression set value reached 56.22%,more than 40%,the indicator does not meet the requirements either.To allow the O-ring to work properly under high and low temperatures for a long time and to ensure that its sealing performance meets the requirements,the Oring performance is targeted to be improved.

    After several rounds of communication with the technical engineers of the Italian joint venture company and the O-ring manufacturer,it was considered that the most important thing was to improve the performance of O-rings at high and low temperatures.However,since-25 ℃is close to the low temperature resistance limit of NBR material,based on the standard durability requirements of the product[47],and at the same time,considering the cost of modification and the cost factor of mass production,it was finally decided to set the modified endurance test time of O-ring at high and low temperature as 5000 h,and the following experiments are designed to verify the rationality of the change,and the experimental protocol is shown in Table 5.

    After normalizing the parameters of the two test scenarios in Table 5 and substituting them into Eq.(3),the predicted average compression set value of the original O-ring at 5000 h can be obtained,as shown in the last column of Table 5.

    Number Factors Time/h Temperature/ ℃ RPM Compression set 1 5000 -25 86 56.58%2 5000 60 86 53.09%

    For the modified O-ring samples,the original dimensions were measured,and some samples were selected to prepare 2 sets of gas meters for testing.According to the modification target,the test time was selected as 5000 h,and high-and low-temperature endurance tests were conducted to verify them.After testing,all tested O-rings rotating dynamic sealing system are not leaking,and the sealing test results meet the requirements of compliance.

    The two sets of meters with the required sealing performance were disassembled,and the test O-rings were removed and stored separately according to the group.Measure the size of the O-ring and calculate according to Eq.(1) to obtain the compressive compression set of the two sets of O-rings,as shown in Table 6.

    t 1 5000 -25 86 42.60% 50%2 5000 60 86 36.68% 40%?

    From Table 6,it can be obtained that the compressive compression set index of modified O-rings was significantly improved.For Scenario 1,the average compression set value of the deflection of the O-ring is 42.30%,which is less than 50%.For Scenario 2,the average compressive compression set value of the Orings is 36.68%,which is less than 40%.The compressive compression set of the O-rings under high and low temperatures meet the requirements,and the improvement has been successful.

    The compression set values obtained from the test are compared with the data of the original O-ring obtained according to the prediction model,and the comparison of compression set before and after improvement is obtained in Table 7.

    Number Compression set after modification Improvement ratio 1 42.30% 56.58% 25.24%2 36.68% 53.09% 30.91%Compression set before modification

    The average compression set value was reduced by 25.24% for Scenario 1 and by 30.91% for Scenario 2.According to the comparison between the test value of compression set and the calculated value,the new Oring sample has been greatly improved compared with the existing O-ring products in terms of comprehensive performance of high and low temperature resistance and wear resistance,and the improvement range is 25% -30%,which is very satisfactory.Finally,the product was tested and put into commercial use,and good results were achieved,which proved that the research results of this study were reasonable and effective.

    4 Conclusions

    Based on the characteristics of gas meters with long service life,wide temperature range and large differences in flow specifications,this paper focuses on the influence of three factors,namely time,temperature and speed,on the sealing performance of O-rings for research and analysis.Based on the fact that compression set is an important index for O-ring performance evaluation and its advantage of being visually observed and measured,it is chosen as the evaluation index for Oring performance in this study.The orthogonal experimental protocol was reasonably designed and multiple experiments were conducted accordingly,and the experimental data were analyzed visually and by ANOVA,the qualitative degree of influence of three main factors on the compression set index was obtained: the temperature factor had the greatest influence,followed by the rotational speed factor,and the time factor had the least influence.After that,regression analysis was carried out on the experimental data to derive the quantitative relationship between the compression set and the three factors,and finally,corresponding experiments were arranged to verify the validity and precision of the relationship.

    Through the analysis of the sealing mechanism of the rotary dynamic sealing system,the finite element simulation analysis of the O-rings in the sealing system,and the empirical study of the orthogonal test,the theory and practice are combined to complete the study of the O-ring rotary dynamic sealing system.And according to the conclusion of the study,the O-ring is modified and optimized as well as further experimental verification.The difficulty of this study lies mainly in the simulation and test part: during the simulation process,O-ring as a nonlinear elastomer,has the characteristics of difficulty of converging the simulation results,especially this test needs to load composite factors,the convergence of results is more difficult; during the test process,the biggest difficulty was the long test time,which accumulated to 49 500 h,using a large amount of equipment resources and test materials.

    Nomenclature

    CfAmount of compression set of the O-ring in compression

    d0O-ring original section diameter

    dfO-ring section diameter after compression

    dcThickness of the O-ring under compression

    SSVariance

    DfDegrees of freedom

    MSMean squared error

    FF-value

    Prob>FP-value

    RRange

    x1Time factorA

    x2Temperature factorB

    x3Speed factorC

    a Constant term

    b1-b3Primary term coefficients

    b4-b9Secondary term coefficients

    ε The model error

    R2Coefficient of determination

    y^tResponse function

    yMean value ofNtrials

    yiTest result

    Appendix

    I Finite element simulation analysis results of Scenarios 2 to 9

    II Experimental instruments

    (1)Endurance test devices are specially designed and manufactured for this study to test the long-lasting sealing performance of O-rings in rotary dynamic sealing systems,as shown in Fig.19.

    (2) The gas meter sealing testing device consists of gas line,pressure gauge,cylinder,lifting mechanism and water tank.The test pressure is adjusted by a manual adjustment knob.The device line is readily available and borrowed when testing is required to check the sealing effect of the O-ring rotary dynamic sealing system after endurance testing.

    (3) Digital projector: Xintian Optoelectronics JT24 Φ300.The shape of the instrument is shown in Fig.20.

    Fig.20 Digital projector

    (4) High and low temperature test chamber:LINPIN instrument is shown in Fig.21.

    Fig.21 High and low temperature test chamber

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